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p with acetyl chloride milled in a ball mill

p with acetyl chloride milled in a ball mill

Theball‐milledcell wall sample (600 mg) was suspended in DMSO (16 ml), and TBAF (2.6 g) was added. A clear solution was formed in 15 min−1.5 h, depending on the sample. Phenol methylation, if desired, could be carried out by simply adding methyl iodide (MeI, 0.7 ml).

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